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]document. Dis- placement of the bromine in 168 by N-Boc-protected 1-amino-2-thiols such as 169 using polymer-supported base 170 (Amberlyst A21) and deprotection with TFA in CH2Cl2 yielded the corresponding imines directly.
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The synthesis of ()-plicamine 188 commenced with the conversion of 4-hydroxyphenylglycine 189 to the amide 190 (see Scheme 33).
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